Brief introduction of Shimadzu liquid chromatograph Main products of Shimadzu liquid chromatograph

I. LC10TVP High Efficiency Liquid

Detectors SPD- 10AVP (ultraviolet-visible) and SPD-M 10AVP (PDA).

RF- 10AXL (fluorescence), RID- 10A (differential refraction), CDD- 10A (conductance) autosamplers SIL- 10ADvp (high efficiency universal analysis), SIL- 10AP.

Column temperature box CTO I 10ACvp, CTO I 10Avp, CT0- 10ASVP.

Combining high pressure, low pressure gradient elution, solution switching and other forms.

Data Processing-Vice President (Workstation)

Data processors C-R7A/C-R8A

Pump type LC-IOADvp micro double plunger LC-IOATv series double plunger

Continuous infusion

The flow setting range is 0.001-5ml/min [1.0-39.2mpa 5.001-9.999ml/min].

The flow accuracy is within 2% or 2 ul/min (whichever is greater).

(0.01-5ml/min (LC-10atvp), 0. 1-5ml/min(LC-IOATvp), 1.0-39.2MPa, in water, at room temperature of 20℃. ..

The flow accuracy is within 0.3% (RSD 0.1%) (0.1-5ml/min, 1.0-39.2mpa, water, room temperature 20℃).

Constant pressure infusion

The pressure setting range is1.0-39.2mpa [0.1MPa step].

The pressure setting accuracy is within the range of 10% or I.OMPa (whichever is greater).

Pressure range high pressure, low pressure

Time, procedure, flow, stress and events. L00P (program duplication). 10 file. The accuracy of 320-segment pressure display is within 2% or 0.5MPa (whichever is greater).

Plunger cleaning LC-IOADvp micro double plunger: it can be automatically cleaned when connected with an automatic cleaning machine (patent number: N02639 130). LC-IOATVP series double plunger: can be connected with syringe or cleaning pump for cleaning.

Size, weight: W260 x H 140 x D420mm, 1 1kg.

The temperature range is 4-35℃

To stabilize the performance of the infusion device, please use a degasser.

Technical specification: SPD- 10AVP

Light source: 10Avp:D2 lamp,10avp (D2 lamp, W lamp).

Wavelength range: 10AVP: 190-600 nm, 10AVVP: 190-900 nm.

Spectral bandwidth: 8 nm

Wavelength accuracy: 1 nm

Wavelength importance 1: 0.lnm

Drift: less than 2 x 10-4AU/h (constant room temperature) (10avp: 250 nm, 10avp: 250 nm, 600 nm, air in the pool).

Soil with noise level below 2:0.35 x 10-5au (equivalent response 2sec) and soil with noise level below 0.5x 10-5au (equivalent response isec) (10avp: 250nm, 10avp: 250 nm, 600nm.

Response: It is equivalent to the time constant of O.05, 0. 1, 0.5, 1.0. 1.5.2.o, 3. o,6。 00.o seconds O.8.O, 65438+65438+.

Range: 0.000 1AUFS step size can be set to 0.00 1-2.56aufs.

Zero adjustment: automatic zero adjustment function, baseline function

Battery (long light path, capacity withstand voltage): 10 mm.8 μ l. 12 MPa (about 120Kgf/cm2) (there are also spare parts to prepare batteries, semi-micro batteries, inert batteries and temperature regulating batteries).

Dual-wavelength simultaneous monitoring: 10 AVP: 190-370 nm or 37 1-600nm.

10AVVP: 190-370 nm or 37 1-700nm, 70 1-900nm, any dual wavelength.

Ratio chromatography: output the set dual-wavelength ratio.

Wavelength scanning function: possible. Wavelength step: 1-5nm 5-segment setting (2-5 nm when using W lamp). 10 nm/sec -5 nm/sec, 5-segment setting (according to wavelength step setting).

Time program: detector body or system controller can be used, including wavelength (2 wavelengths), auto-zero, range, symbol indication, response, wavelength scanning, event polarity, on/off and cycle (program cycle).

Polarity conversion: can

Output: recorder output: 10mv terminal integrator output: 5, 1.2.4, 1.25, 2.5 Au/V6 segment switching.

In dual-wavelength mode, the chromatographic axis on the ch 1 side is absent.

Size and weight: W260 x H 140 x IM20mm, 13kg.

Working environment temperature range: 4-35℃

1: Single wavelength power supply on time, indicating the importance of wavelength change.

2: Dual Wavelength Mode

main feature

1 A new generation of high reliability and high efficiency LC-VP series improves the reliability and durability of hardware. In order to improve the analysis efficiency, the continuous analysis ability and safety measures of multiple samples are enhanced.

2 Flexibility and Extensibility LC-VP series consists of various high-performance devices. While adding new functions to each unit, we should pay attention to the compatibility with the old models. Therefore, the most suitable system can be formed according to the needs of customers (analysis purpose, budget, existing model). LC-VP series has flexible scalability, from semi-micro analysis and routine analysis to semi-preparation and preparation system. In data processing, we can flexibly choose a new generation of 32-bit workstations CLASS-VP6. 1 or a simple data processor.

3. Fully support GLP/GMP to provide various documents such as adaptability certificate, operation guide to confirm effectiveness required in IS0900 1 quality management, as well as system check and system stability calculation software. Each unit of LC-VP series has new VP function, which realizes efficient daily validity test. Provide users with comprehensive support, from regular inspection of equipment including old models to providing effective analysis methods, holding technical exchanges and training courses.

Instrument introduction

expand on

1 A new generation of high reliability and high efficiency LC-VP series improves the reliability and durability of hardware. In order to improve the analysis efficiency, the continuous analysis ability and safety measures of multiple samples are enhanced.

2 Flexibility and Extensibility LC-VP series consists of various high-performance devices. While adding new functions to each unit, we should pay attention to the compatibility with the old models. Therefore, the most suitable system can be formed according to the needs of customers (analysis purpose, budget, existing model). LC-VP series has flexible scalability, from semi-micro analysis and routine analysis to semi-preparation and preparation system. In data processing, we can flexibly choose a new generation of 32-bit workstations CLASS-VP6. 1 or a simple data processor.

3. Fully support GLP/GMP to provide various documents such as adaptability certificate, operation guide to confirm effectiveness required in IS0900 1 quality management, as well as system check and system stability calculation software. Each unit of LC-VP series has new VP function, which realizes efficient daily validity test. Provide users with comprehensive support, from regular inspection of equipment including old models to providing effective analysis methods, holding technical exchanges and training courses.

Transfusion pumps LC- 10ADvp, LC-10advp.

Detectors SPD- 10AVP (ultraviolet-visible) and SPD-M 10AVP (PDA).

RF- 10AXL (fluorescence), RID- 10A (differential refraction) and CDD- 10A (conductance).

Automatic sampler SIL- 10ADvp (high-performance universal analysis), SIL- 10AP (preparation and quality injection), SIL-HT (high efficiency) and SIL- 10AF (with pretreatment function).

Column temperature box CTO I 10ACvp, CTO I 10Avp, CT0- 10ASVP.

Combining high pressure, low pressure gradient elution, solution switching and other forms.

Data Processing-Vice President (Workstation)

Data processors C-R7A/C-R8A

Pump type LC-IOADvp micro double plunger LC-IOATv series double plunger

Continuous infusion

The flow setting range is 0.001-5ml/min [1.0-39.2mpa 5.001-9.999ml/min].

The flow accuracy is within 2% or 2 ul/min (whichever is greater).

(0.01-5ml/min (LC-10atvp), 0. 1-5ml/min(LC-IOATvp), 1.0-39.2MPa, in water, at room temperature of 20℃. ..

The flow accuracy is within 0.3% (RSD 0.1%) (0.1-5ml/min, 1.0-39.2mpa, water, room temperature 20℃).

Constant pressure infusion

The pressure setting range is1.0-39.2mpa [0.1MPa step].

The pressure setting accuracy is within the range of 10% or I.OMPa (whichever is greater).

Pressure range high pressure, low pressure

Time, procedure, flow, stress and events. L00P (program duplication). 10 file. A total of 320 paragraphs.

The accuracy of pressure display is within 2% or 0.5MPa (whichever is greater).

Plunger cleaning LC-IOADvp micro double plunger: it can be automatically cleaned when connected with an automatic cleaning machine (patent number: N02639 130). LC-IOATVP series double plunger: can be connected with syringe or cleaning pump for cleaning.

Size, weight: W260 x H 140 x D420mm, 1 1kg.

The temperature range is 4-35℃

To stabilize the performance of the infusion device, please use a degasser.

Technical specification: SPD- 10AVP

Light source: 10Avp:D2 lamp,10avp (D2 lamp, W lamp).

Wavelength range: 10AVP: 190-600 nm, 10AVVP: 190-900 nm.

Spectral bandwidth: 8 nm

Wavelength accuracy: 1 nm

Wavelength importance 1: 0.lnm

Drift: less than 2 x 10-4AU/h (constant room temperature) (10avp: 250 nm, 10avp: 250 nm, 600 nm, air in the pool).

Soil with noise level below 2:0.35 x 10-5au (equivalent response 2sec) and soil with noise level below 0.5x 10-5au (equivalent response isec) (10avp: 250nm, 10avp: 250 nm, 600nm.

Response: It is equivalent to the time constant of O.05, 0. 1, 0.5, 1.0. 1.5.2.o, 3. o,6。 00.o seconds O.8.O, 65438+65438+.

Range: 0.000 1AUFS step size can be set to 0.00 1-2.56aufs.

Zero adjustment: automatic zero adjustment function, baseline function

Battery (long light path, capacity withstand voltage): 10 mm.8 μ l. 12 MPa (about 120Kgf/cm2) (there are also spare parts to prepare batteries, semi-micro batteries, inert batteries and temperature regulating batteries).

Dual-wavelength simultaneous monitoring: 10 AVP: 190-370 nm or 37 1-600nm.

10AVVP: 190-370 nm or 37 1-700nm, 70 1-900nm, any dual wavelength.

Ratio chromatography: output the set dual-wavelength ratio.

Wavelength scanning function: possible. Wavelength step: 1-5nm 5-segment setting (2-5 nm when using W lamp). 10 nm/sec -5 nm/sec, 5-segment setting (according to wavelength step setting).

Time program: detector body or system controller can be used, including wavelength (2 wavelengths), auto-zero, range, symbol indication, response, wavelength scanning, event polarity, on/off and cycle (program cycle).

Polarity conversion: can

Output: recorder output: 10mv terminal integrator output: 5, 1.2.4, 1.25, 2.5 Au/V6 segment switching.

In dual-wavelength mode, the chromatographic axis on the ch 1 side is absent.

Size and weight: W260 x H 140 x IM20mm, 13kg.

Working environment temperature range: 4-35℃

1: Single wavelength power supply on time, indicating the importance of wavelength change.

2: Dual Wavelength Mode

Second, LC20A original liquid chromatograph

Shimadzu LC-20A liquid chromatograph series is one of the most stable liquid chromatograph models developed by Shimadzu Company in the world. The infusion set Prominence LC-20AD/20AT/20AB is flexible in configuration, meeting customers with different needs, and its function and stability are superior to LC- 10A and 15C.

LC-20AD

Infusion mode: parallel double plunger

Plunger capacity: 10ul

Maximum discharge pressure: 40MPa

Flow setting range: 0.000 1 ml/min-10.0000 ml/min.

Flow accuracy: 1% or 0.5ul /min, which is within a larger value (0.0 1mL/min-2mL/min).

Flow accuracy: less than 0.3 (RSD: less than 0. 1%)

LC-20AT

Infusion mode: Double plungers in series.

Plunger capacity: main pump head 47ul, auxiliary pump head 23ul.

Maximum discharge pressure: 40MPa

Flow setting range: 0.00 1 ml/min-10.000 ml/min.

Flow accuracy: 2% or 2uL/min, whichever is greater (0.0 1 ml/min -5 ml/min).

Flow accuracy: less than 0.3 (RSD: less than 0. 1%)

LC-20AB

Infusion mode: parallel double plunger (type 2)

Plunger capacity: 10uL

Maximum discharge pressure: 40MPa

Flow setting range: 0.000 1 ml/min-10.0000 ml/min.

Flow accuracy: 1% or 0.5uL/min, which is within a larger value (0.0 1mL/min-2mL/min).

Flow accuracy: less than 0.3 (RSD: less than 0. 1%)

Gradient system

LC-20AB

Gradient mode: high pressure mixing

Number of mixed solvents: 2 liquids

Accuracy of mixed concentration: less than 0.5%

LC-20AD/20AT high voltaGE ge specification

Gradient mode: high pressure mixing

Number of mixed solvents: 2 or 3 liquids.

Accuracy of mixed concentration: less than 0.5% (LC-20AD) and less than 1% (LC-20AT).

LC-20AD/20AT low voltaGE ge specification

Gradient mode: low pressure mixing

Number of mixed solvents: 4 liquids at most.

Accuracy of mixed concentration: less than 0.5% (LC-20AD) and less than 1% (LC-20AT).

Ultraviolet visible detector

SPD-20A/20AV ultraviolet-visible detector for prominence

Prominences SPD-M20PDA detector

SPD-20A / SPD-20AV

Light source: SPD-20A D2 lamp, SPD-20AV D2 lamp, tungsten lamp.

Number of diode components: None

Wavelength range: SPD-20A 190nm-700nm, SPD-20AV 190nm-900nm.

Spectral bandwidth? Gap width: 8 nm

Wavelength accuracy: less than 65438 0 nm

Wavelength accuracy: below 0. 1nm.

Noise: 0.25× 10-5au (under specific conditions)

Drift: 1× 10-4AU/h (under certain conditions)

Linearity: 2.5AU(ASTM specification)

Functions: 190nm-370nm or more dual wavelength detection, proportional chromatographic output, wavelength scanning.

Battery: light path length: 10mm, capacity: 12mL, voltage resistance: 12MPa.

SPD-M20A

Light source: D2 lamp, incandescent lamp

Number of diode elements: 5 12

Wavelength range:190nm-800nm

Spectral bandwidth? Gap width: 1.2 nm (high resolution mode) 8 nm (high sensitivity mode)

Wavelength accuracy: less than 65438 0 nm

Wavelength accuracy: below 0. 1nm.

Noise: 0.3× 10-5au (under specific conditions)

Drift: 0.5× 10-3AU/h (under specific conditions)

Linearity: 2.0AU(ASTM specification)

Functions: contour output, spectral retrieval, maximum output

Battery: light path length: 10mm, capacity: 10mL, voltage resistance: 12MPa.

Automatic sampler highlights SIL-20A/20AC

Injection mode: full injection, variable injection quantity.

Setting range of sampling volume: 0. 1ul- 100ul (standard) and 1ul -2.000mL (optional).

Number of samples processed:

175( 1 ml sample bottle)

105 (1.5ml sample bottle) (sil-20ac70 (1.5ml sample bottle))

50(4 ml sample bottle)

192(96-hole MTP 2 area)

768(384-hole MTP 2 block)

In addition to the above specifications, 1.5mL sample bottles can be used.

Accuracy of injection volume: less than 65438 0%

Precision of injection amount: RSD: less than 0.3% (under the specified conditions of injection 10mL).

Cross contamination: less than 0.005% (naphthalene, chlorhexidine)

Repeated sampling times: 30/ 1 sample at most.

Needle cleaning: set at will before and after injection.

Sample cooler: SIL-20A does not have the cooling and heating mode of SIL-20AC module, but also has the dehumidification function of 4℃-4℃.